AC-55541_LCMS_13693_MedChemExpress

MS Report from Instrument: LCMS-02 File ..7-2 2017-07-07 15-32-44\\CPK2017-707-13693.D Tgt Mass (CHM): Injection Date : 7 Jul 17 6:16 pm +0800 Seq. Line : 37 Sample Name : CPK2017-707-13693 Location : P1-E-06 Acq. Operator : ZLJ_587 Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\chem32\\1\\DATA\\20170707\\20170707-2 2017-07-07 15-32-44\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\DATA\\20170707\\20170707-2 2017-07-07 15-32-44\\1-POS-3MIN.M Catalog No : HY-14350 Batch#13693 A-RP-186 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 B, Sig=214,4 Ref=off 1.7811.2881.6581.730mAU1500100050000.5 DAD1 C, Sig=254,4 Ref=off mAU60040020000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 702000001500001000005000000.511.5 Ion 519.4, MSD1 519.4,Target Mass 518.4 +H Positive, EIC=519.1:520.1 30000200001000000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.522.5min11..8801271.7731.51.6651.73111.51.78122.5min22.5min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.29 0.02 6.84 0.19 0.23 157 1.66 0.02 6.58 0.06 0.22 ND 1.73 0.02 5.83 4.02 0.20 ND 1.78 0.03 2925.22 1861.15 99.35 518 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.67 0.02 2.96 0.10 0.23 ND 1.73 0.02 2.39 1.65 0.18 ND 1.78 0.03 1304.90 838.71 99.59 518 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.77 0.04 183651.64 1433.15 100.00 518LCMS-02 7/13/2017 18:13:16 ZLJ_587Page 1 of 2

MS Report from Instrument: LCMS-02Ret. Time: 1.77 <<<< POSITIVE SPECTRA >>>> ES-API Positive12000100008000 521.06000400020000200300400500600700800900m/z 520.0LCMS-02 7/13/2017 18:13:16 ZLJ_587Page 2 of 2