Bilastine_LCMS_13390_MedChemExpress

MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\CPK\\CPK2017-216-13390.D Tgt Mass (EZX): 463.60 Injection Date : 16-Feb-17, 14:50:03 Seq. Line : 0 Sample Name : CPK2017-216-13390 Location : P1-E-05 Acq. Operator : GZZ_718 Inj : 0 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\SIM-HM-174C_005-H01GI03(0.0.05%TFA).M Catalog No : HY-14447 Batch#13390 Easy-Access Method: '1-POS-3MIN' 463.60 Method Info : Postive,MS:100-1000,Column ID:A-RP-85,50℃ DAD1 B, Sig=214,4 Ref=off 1.2561.209mAU60040020000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 703000002500002000001500001000005000000.511.5 Ion 464.6, MSD1 464.6,Target Mass 463.6 +H Positive, EIC=464.3:465.3 17500015000012500010000075000500002500000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.30522.5min1.3031.522.5min1.4051.4381.48511..5568131.6401.6711.6941.7221764691..71.80011..8823081.8621.90311..9924842.0182.0692.1032.12702.1682.2112.2392.2742.3122.3332.3462.36122..4424132.4882.5181.522.5 RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.21 0.02 1.19 1.29 0.05 ND 1.26 0.05 2381.47 826.61 99.95 464HY-LCMS-02 2/16/2017 3:19:44 PM GZZ_718Page

2..66202622.6672..77109522.7812..88203522.8612.8912.9312.992min1 of 2

MS Report from Instrument: HY-LCMS-02

Ret. Time: 1.30 <<<< POSITIVE SPECTRA >>>> ES-API Positive 232.850000400003000020000100000200 466.4 465.3 464.3300400500600700800900m/zHY-LCMS-02 2/16/2017 3:19:44 PM GZZ_718Page 2 of 2