Ademetionine_MS_17102_MedChemExpress

Data File D:\\AGLIENT 1260\\DATA\\20150721\\20150721 2015-07-21 09-32-38\\BIZ2015-721-DJL1.DSample Name: BIZ2015-721-DJL1=====================================================================Acq. Operator : Li Shan(LCMS-02) Seq. Line : 22Acq. Instrument : HY-LCMS-02 Location : P1-C-02Injection Date : 7/21/2015 11:06:12 AM Inj : 1 Inj Volume : 3.000 µlAcq. Method : D:\\AGLIENT 1260\\DATA\\20150721\\20150721 2015-07-21 09-32-38\\100-1000MS+3MIN- 1.5_(0.02%FA).MLast changed : 7/21/2015 9:32:39 AM by Li Shan(LCMS-02)Analysis Method : D:\\AGLIENT 1260\\DATA\\20150709\\20150709 2015-07-09 09-04-13\\100-1000MS+3MIN- 1.5_(0.02%FA).M (Sequence Method)Last changed : 7/21/2015 1:06:26 PM by Li Shan(LCMS-02) (modified after loading)Method Info : Postive,MS:100-1000,Column ID:A-RP-132,40℃ Catalog No : HY-B0617 Batch#17102 A-RP-134 Additional Info : Peak(s) manually integrated MSD1 TIC, MS File (D:\\AGLIENT 1260\\DATA\\20150721\\20150721 2015-07-21 09-32-38\\BIZ2015-721-DJL1.D) ES-API, Pos, Sca 0.3884000003500003000002500002000001000005000000.511.522.53min 1.453150000 HY-LCMS-02 7/21/2015 1:06:28 PM Li Shan(LCMS-02)Page 1 of 2

Data File D:\\AGLIENT 1260\\DATA\\20150721\\20150721 2015-07-21 09-32-38\\BIZ2015-721-DJL1.DSample Name: BIZ2015-721-DJL1MS Signal: MSD1 TIC, MS File, ES-API, Pos, Scan, Frag: 50 Spectra averaged over upper half of peaks. Noise Cutoff: 1000 counts. Reportable Ion Abundance: > 10%. Retention Mol. WeightTime (MS) MS Area or Ion 0.388 1736492 399.10 I 298.10 I 200.10 I 102.10 I 1.453 273701 299.10 I 298.10 I 258.15 I*MSD1 SPC, time=0.359:0.414 of D:\\AGLIENT 1260\\DATA\\20150721\\20150721 2015-07-21 09-32-38\\BIZ2015-721-DJL1.D ES-API,100806040200100200300400500600700800900m/z 200.1Max: 169286 102.1 298.1*MSD1 SPC, time=1.434:1.489 of D:\\AGLIENT 1260\\DATA\\20150721\\20150721 2015-07-21 09-32-38\\BIZ2015-721-DJL1.D ES-API,1412108 190.020100 300.14 258.16 298.1 400.1 399.1200300400500600700800900m/z *** End of Report ***HY-LCMS-02 7/21/2015 1:06:28 PM Li Shan(LCMS-02)Page 2 of 2