Sulfanitran_LCMS_22617_MedChemExpress

MS Report from Instrument: HY-LCMS-02 File D:\\CHEM32\\1\\DATA\\BIZ\\BIZ2016-N25-WJ6.D Tgt Mass (EZX): 335.00 Injection Date : 25 Nov 16 11:40 am +0800 Seq. Line : 0 Sample Name : BIZ2016-N25-WJ6 Location : P1-D-06 Acq. Operator : KFF(LCMS-02) Inj : 1 Spec. Reported : MS Integration Inj Volume : 1 ul Acq. Method : D:\\Chem32\\1\\METHODS\\1-POS-3MIN.M Analysis Method : D:\\CHEM32\\1\\METHODS\\1-POS-3MIN-PROSRSS.M Catalog No : HY-B0947 Batch#22617 Easy-Access Method: '1-POS-3MIN' 335.00 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C*DAD1 B, Sig=214,4 Ref=off mAU60040020000.5*DAD1 C, Sig=254,4 Ref=off mAU60040020000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.51.6471.8161.99311.51.6531.7971.65322.5min*22.5min*400002000000.511.5 Ion 336, MSD1 336,Target Mass 335 +H Positive, EIC=335.7:336.7 200001500010000500000.5 Integration Results for DAD1 B, Sig=214,4 Ref=off11.521.6492.5min22.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.65 0.02 872.69 742.10 99.75 336 1.80 0.03 2.14 0.67 0.25 233 Integration Results for DAD1 C, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.65 0.02 865.65 746.93 99.60 336 1.82 0.03 1.47 0.79 0.17 233 1.99 0.02 1.97 1.51 0.23 233HY-LCMS-02 11/25/2016 12:00:48 KFF(LCMS-02)Page 1 of 2

MS Report from Instrument: HY-LCMS-02

Ret. Time: 1.65 <<<< POSITIVE SPECTRA >>>> ES-API Positive 336.1 233.2 141.1 338.2 374.180006000400020000200300400500600700800900m/zHY-LCMS-02 11/25/2016 12:00:48 KFF(LCMS-02)Page 2 of 2